Wide-field hyperspectral camera gives researchers a real-time window into single-nanoparticle electrochemistry
Peer-Reviewed Publication
Updates every hour. Last Updated: 25-Oct-2026 14:16 ET (25-Oct-2026 18:16 GMT/UTC)
Researchers have developed a wide-field Fourier transform hyperspectral imaging system that captures electrochemical reactions on hundreds of individual nanoparticles simultaneously. By integrating a common-path interferometer with a fast 2D camera, the method provides real-time spectral evolution during electrodeposition of palladium and cadmium sulfide on gold nanoparticles. Statistical analysis reveals distinct deposition behaviors on nanospheres versus nanorods—insights that would require thousands of tedious single-particle measurements using conventional approaches.
Ammonia is essential for fertilizers and is emerging as a zero‑carbon energy carrier, but its industrial production via the Haber‑Bosch process is energy‑intensive and emits large amounts of CO2. Meanwhile, nitrate pollution from agriculture and industry has contaminated groundwater worldwide, threatening ecosystems and human health. Electrocatalytic nitrate reduction to ammonia (NO3RR) offers an elegant solution: using renewable electricity to convert nitrate waste into valuable ammonia.
Hyperbolic phonon polaritons (HPhPs) are hybrid light–matter waves that can confine infrared electromagnetic fields to spatial scales far below the corresponding free-space wavelength. Controlling HPhPs on femtosecond timescales could provide a foundation for future ultrafast and ultracompact nanophotonic devices. However, directly imaging such ultrafast dynamics has remained challenging because HPhPs are strongly dispersive and their wavelength changes markedly with frequency. Broadband femtosecond laser pulses therefore excite HPhPs over a range of wavelengths, causing their interference patterns to overlap and wash out in real-space images. In this study, researchers developed an ultrafast infrared near-field optical microscopy technique that combines nanoscale spatial resolution and an approximately 150-femtosecond temporal resolution with a spectral resolution of about 10 cm⁻¹. By using a diffraction grating to spectrally resolve the light scattered from the microscope tip before detection, the technique enables frequency-selective imaging without sacrificing ultrafast time resolution. Applying the new technique to a van der Waals heterostructure composed of tungsten disulfide (WS2) and hexagonal boron nitride (hBN), the researchers revealed how photoexcited charge carriers generated in WS2 transiently modulate HPhPs propagating in the adjacent hBN. The researchers observed changes in the HPhP electric-field amplitude and, in structures containing a relatively thick WS₂ layer, a change in the HPhP wavelength. The researchers say, “The results establish a new platform for observing and controlling nanoscale light propagation on femtosecond timescales, opening new opportunities for ultrafast nanophotonics”.
POSTECH research team develops a highly directional speaker by integrating metamaterials with a single ultrasonic transducer.
A new way to imprint complex surfaces on low-cost, sustainable polymers could be used in a wide range of industries, including for water-repellent coatings, optical devices and data storage discs.
The complex nano- and micro-scale patterns on sulfur-derived polymers, unveiled this week in the American Chemical Society ACS Applied Materials and Interfaces journal, build on a wide range of green chemistry solutions led by Flinders University.